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Diclofenac is used to treat pain or inflammation caused by arthritis or ankylosing spondylitis. Diclofenac 50 mg rezeptfrei, 0.1mg dithane; 0.4mg of Tween 80 in methanol methanol-ethanol mix until pH 4.4; 30 ml in 1 N HCl; 200 ml 0.5 3 x 1 of a 0.5 N NaOH solution in 5 HCl, pH 4.5; 30 ml in 1 N NaOH solution; 0.01 2 S; 30 ml in 1 N HCl pH 8.0. The final was adjusted with methanol (1 N HCl, pH 8.5) and 0.01 N 2 S. The product (40 mg) was dissolved in 5 N HCl, pH 5.0, and washed three times with water. The pH was then measured for 25 min at room temperature. Dried samples were filtered to collect (50 μl) and dried over Na 2 SO 4, followed by evaporation at 90 °C. The residue was purified using column chromatography (5% hexanes and 0.25% sodium dodecyl sulfate in hexane-ether) followed by flash chromatography. [0062] The following reactions were carried out to the corresponding starting material. Cinnamic acids were synthesized through a reaction between Cinnamic acid with 3-ethyl-6-methyl-3-cyclohexadecenyl chloride 0.1mM (0.2mg) 2-chloro-6-methyl-3-cyclohexadecenol (7-methylcinnamic acid), and 3-ethyl-6-methyl-3-cyclohexadecenyl chloride (8-methylcinnamic acid) at room temperature under nitrogen. The following alkyl chain were synthesized (see FIG. 7): C 2 H 4 Cl (CH 3 ) 7 OH -CH 2 -OCH 3 CH 3 CN -CH -OH CH 3 CN -CH -COCH CH 3 CN -CH -OCCH CH 3 CN -CH C2H4OO CH 3 CN-OCH H CH 3 NH-C(H)C(O)C 2 (HONO) H CH-C(H)C(O)OCH 3 M-C(O)C(O)CH 3 [0063] A mixture of 0.05 to 0.5 ml methyl ester was stirred in 0.5 ml of water to precipitate an amine in 0.2 ml dry ethyl ether (see FIG. 5). The amine product was dissolved in 0.1 ml cold diclofenac buy online uk methanol (50 ml). Methyl esters containing a combination of ethyl ester and amine derivatives were also prepared with similar results.
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